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Understanding the Principles of Organic Chemistry: A Laboratory Course

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ÁöÀºÀÌ :  Pedersen, Myers
¹ßÇàÀÏ :  2011 ³â
ISBN :  9781111428174
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Part I. Theory and Techniques
1. Sarety in the Chemistry Laboratory
2. The Laboratory Notebook and the Laboratory Period
3. Where to Find It: Searching the Literature
4. Things You Need to Know Before You Begin
5. Properties of Organic Molecules
6. Characteristic Physical Properties of Pure Compounds
7. Isolation and Purification of Compounds
8. Structure Determination
9. Running a Synthetic Reaction
Part II. The Experiments
Experiment 1. Calibrating a Pasteur Pipette
Experiment 2. Investigating Solubility and Acid-Base Reactions
Experiment 3. Mixed Melting Points
Experiment 4. Whittling Down the Possibilities: Identifying an Unknown Using Molecular Dipole Moment, Solubility, Density and Boiling Point Data
Experiment 5. Recrystallization and Melting Points: Recrystallization of Adipic and Salicylic Acids
Experiment 6. Recrystallization and Melting Points: Recrystallization of an Unknown Solid and the Decolorization of Brown Sugar
Experiment 7. Thin Layer Chromatography (TLC)
Experiment 8. Identification of an Adulterated Herb or Spice by Thin Layer Chromatography (TLC)
Experiment 9. What Do You Take for Pain?
Experiment 10. Nucleophilic Substitution Reactions of Alkyl Halides
Experiment 11. The Isolation of Trimyristin from Nutmeg
Experiment 12. The Magtrieve¢â Oxidation of 4-Chlorobenzyl Alcohol
Experiment 13. The Sodium Borohydride Reduction of Benzil and Benzoin
Experiment 14. The Grignard Reaction: The Preparation of 1,1-Diphenylethanol
Experiment 15. The Asymmetric Dihydroxylation of trans-Stilbene
Experiment 16. Some Chemistry of Oxide
Experiment 17. A Dehydrogenation/Hydrogenation Reaction
Experiment 18. The Friedel-Crafts Reaction
Experiment 19. Microwave Heating of Organic Compounds
Experiment 20. The Reaction of 1,1-Diphenylethanol on Clay in the Presence of Microwave Radiation
Experiment 21. The Wittig Reaction
Experiment 22. The Suzuki Reaction
Experiment 23. The Crossed-Aldol Condensation
Experiment 24. Identifying the Structure of an Aldehyde by Qualitative Analysis
Experiment 25. The Benzoin Reaction
Experiment 26. The Diels-Alder Reaction
Experiment 27. -©¬-Unsaturated Carboxylic Acid Derivative.
Experiment 28. The Reaction of 2-Acetylphenyl Benzoate with Potassium Hydroxide
Experiment 29. The Reaction of 2-Acetylphenyl Benzoate with Potassium Hydroxide
Experiment 30. Synthesis of 1,2,3,4-Tetrahydro-?-Carboline
Experiment 31. Base-Catalyzed Hydrolysis of Nicotinonitrile Using an Anion-Exchange Resin
Experiment 32. Reactions of Salicylamide
Experiment 33. The Hunsdiecker Reaction
Experiment 34. The Investigation of the Mechanism of a Reaction
Experiment 35. Monoterpenes and the Ritter Reaction
Experiment 36. Chemoselectivity in Transfer-Hydrogenation Reactions